TY - JOUR PY - 2013// TI - SPME-GC-MS analysis of α-pyrrolidinovaleorophenone in blood in a fatal poisoning case JO - Forensic toxicology A1 - Saito, Takeshi A1 - Namera, Akira A1 - Osawa, Motoki A1 - Aoki, Hiromichi A1 - Inokuchi, Sadaki SP - 328 EP - 332 VL - 31 IS - 2 N2 - We provided toxicological analytical support for a fatal case of abuse of α-pyrrolidinovaleorophenone (α-PVP) -- a stimulant compound with an affect similar to the designer drug MDPV. Solid-phase microextraction (SPME) and capillary gas chromatography coupled to mass spectrometry (GC-MS) was employed to quantify the drug in whole blood. The whole blood concentration of the drug in the heart was 486 ng/ml. This is the first report of α-PVP intoxication as ascertained by mass spectrometric identification of α-PVP in whole blood.

Language: en

LA - en SN - 1860-8965 UR - http://dx.doi.org/10.1007/s11419-013-0183-8 ID - ref1 ER -