TY - JOUR PY - 2016// TI - Identification and characterization of new designer drug 4-fluoro-PV9 and α-PHP in the seized materials JO - Forensic toxicology A1 - Majchrzak, Milena A1 - Rojkiewicz, Marcin A1 - Celiński, Rafał A1 - Kuś, Piotr A1 - Sajewicz, Mieczysław SP - 115 EP - 124 VL - 34 IS - N2 - In this study, we present identification and physicochemical characterization of new cathinone derivatives, 4-fluoro-PV9 and already known α-PHP in seized materials. Although the disclosure of α-PHP from an illegal product had been reported and characterized to some extent, the data on α-PHP are also presented together with those of 4-fluoro-PV9. The data of characterization for the two compounds were obtained by high-performance liquid chromatography (HPLC)-mass spectrometry and HPLC-diode array detection, electrospray ionization/ion trap mass spectrometry in MS(2) and MS(3) modes, gas chromatography-mass spectrometry, thermogravimetric analysis, differential scanning calorimetry, Fourier transform infrared spectroscopy, ultraviolet-visible spectroscopy, and nuclear magnetic resonance spectroscopy. To our knowledge, this is the first report for identification and detailed characterization of 4-fluoro-PV9 circulated on the illegal drug market.

Language: en

LA - en SN - 1860-8965 UR - http://dx.doi.org/10.1007/s11419-015-0295-4 ID - ref1 ER -