TY  - JOUR
PY  - 2016//
TI  - Detection of fipronil in postmortem samples by LCMS using solid phase extraction
JO  - Indian journal of forensic medicine and toxicology
A1  - Jameela, S.R.
A1  - Joseph, S.
A1  - Sivadasan, K.G.
A1  - Thankamany, V.C.
SP  - 60
EP  - 62
VL  - 10
IS  - 2
N2  - A specific method to detect fipronil in postmortem samples with solid phase extraction is presented. For sample clean up a simple but selective solid phase extraction is chosen. Elution was done with 1:1 mixture of dichloromethane and ethyl acetate. Fipronil was detected in stomach tissue and in blood sample. For LCMS gradient elution with a mixture of acetonitrile and water was used. The column was Hypersil Gold. This method is applied to a suicidal case involving intoxication with Fipronil. © 2016, Indian Journal of Forensic Medicine and Toxicology. All rights reserved.<p /> <p>Language: en</p>
LA  - en
SN  - 0973-9122
UR  - http://dx.doi.org/10.5958/0973-9130.2016.00063.3
ID  - ref1
ER  -